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Beilstein J. Org. Chem. 2017, 13, 806–816, doi:10.3762/bjoc.13.81
Graphical Abstract
Figure 1: Collidine-assisted vs DMAP-assisted N-methylation process on solid support. (A) Collidine-assisted ...
Figure 2: Motifs 1–5 were used as models for the optimization of the N-methylation process. i) Introduction o...
Figure 3: Sulfonylation optimization study. HPLC trace overlay that shows the sulfonylation of motif 4 to yie...
Figure 4: DFT calculations for the reaction of o-NBS-Cl with a) collidine and b) DMAP. The structure of the r...
Figure 5: Methylation of motif 3a to 3b using various reaction conditions. HPLC trace overlay presents the ef...
Figure 6: Optimization of o-NBS removal reaction conditions demonstrated on motif 5b. HPLC trace overlay of i...
Figure 7: HPLC trace overlay and MS analysis of the somatostatin analogue, 1SW-1, which was Nα-methylated on ...